1,2-双(二甲氧基磷基)-苯合成路线 (共 4 条)
反应条件
T=60°C; Irradiation;
参考文献
Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Yin, Ping
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , p. 3925 - 3932
参考文献
Seyferth,D.; Paetsch,J.D.H.
Journal of Organic Chemistry, 1969 , vol. 34, # 5 p. 1483 - 1484
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C;
参考文献
Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Yin, Ping
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , p. 3925 - 3932
反应条件
1: 79 percent / lithium aluminium hydride / tetrahydrofuran / 20 °C
2: 90 percent / 1.) nBuLi / 1.) n-hexane, ether, -35 deg C, 1 h; 2.) 25 deg C, 2 h
View Scheme
参考文献
Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Yin, Ping
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , p. 3925 - 3932