1-乙酰氧基-1,3-丁二烯合成路线 （共 41 条）
反应条件
laccase in acetate buffer
T=55°C; Diels-Alder reaction; pH=4.5; 24 h;
参考文献
Witayakran, Suteera; Zettili, Abdullah; Ragauskas, Arthur J.
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 2983 - 2987
反应条件
laccase in acetate buffer
T=3 - 20°C; Diels-Alder reaction; pH=4.5; 24 h;
参考文献
Witayakran, Suteera; Zettili, Abdullah; Ragauskas, Arthur J.
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 2983 - 2987
反应条件
(i) THF, (ii) /BRN= 1743394/, toluene, (iii) HgO, H2SO4, acetone; Multistep reaction;
参考文献
Krohn; Tolkiehn
Chemische Berichte, 1979 , vol. 112, # 10 p. 3453 - 3471
参考文献
Amin, Shantu; Huie, Keith; Hussain, Nalband; Balanikas, George; Carmella, Steven G.; Hecht, Stephen S.
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1206 - 1211
反应条件
hydroquinone in benzene
参考文献
Holtz,H.D.; Stock,L.M.
Journal of the American Chemical Society, 1964 , vol. 86, p. 5183 - 5188
反应条件
hydroquinone in xylene
24 h; Heating;
参考文献
Rice, Joseph E.; LaVoie, Edmond J.; Hoffmann, Dietrich
Journal of Organic Chemistry, 1983 , vol. 48, # 14 p. 2360 - 2363
反应条件
2: THF; LiAlH4; diethyl ether
3: aqueous methanol. H2SO4 / Erhitzen des jeweils erhaltenen Reaktionsprodukts mit Acetanhydrid und Pyridin
View Scheme
参考文献
Inhoffen et al.
Croatica Chemica Acta, 1957 , vol. 29, p. 329,337
反应条件
3 A molecular sieve in ethylene glycol dimethyl ether
T=25°C; 120 h;
参考文献
Schmidt, Richard R.; Vogt, Klaus
Synthesis, 1983 , # 10 p. 799 - 801
反应条件
3 A molecular sieve in dichloromethane
T=25°C; 144 h; Yield given. Yields of byproduct given;
参考文献
Schmidt, Richard R.; Vogt, Klaus
Synthesis, 1983 , # 10 p. 799 - 801
参考文献
Bailey; Baylouny
Journal of the American Chemical Society, 1959 , vol. 81, p. 2126,2128
