(R)-(+)-1-苯基乙醇合成路线 (共 353 条)
反应条件
3 A molecular sieve; β-galactosidase in dimethyl sulfoxide T=55°C; 4 h; Product distribution; Further Variations:ReagentsSolventsdifferent formulations of enzyme;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 18, # 1 p. 124 - 128
反应条件
methanol; (CH3N2C3H2CHNC6H10NHSO2C6H4CH3)ZnCl2; sodium methylate in methanol-d4; dichloromethane-d2; acetonitrile-D3 Kinetics;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 339, # 1-2 p. 72 - 78
反应条件
96 h; by Spirodela oligorrhiza; Title compound not separated from byproducts;
参考文献
Phytochemistry (Elsevier), , vol. 26, # 4 p. 1001 - 1004
反应条件
2BH3*NH2CH2CH2NH2 in solid enantioselective reduction of var. ketones in optically active host compounds with a BH3-ethylenediamine complex in the solid state; Product distribution;
参考文献
Toda, Fumio; Mori, Koji
Journal of the Chemical Society, Chemical Communications, 1989 , # 17 p. 1245 - 1246
反应条件
sodium tetrahydroborate in solid 120 h; Ambient temperatureother variant: ultrasonic irradiation, 2 d; Product distribution;
参考文献
Carbohydrate Research, , vol. 192, p. 363 - 365
反应条件
Candida antarctica lipase T=80°C; 0.25 h; Irradiationwithout MW irradiation; other reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 22 p. 7746 - 7749
反应条件
T=0°C; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4869,4872
参考文献
Journal of the American Chemical Society, , vol. 77, p. 6261,6262
反应条件
ee = 96percent; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 24, # 42 p. 4581 - 4584
反应条件
phosphate buffer; Pseudomonas lipase Amano AH; (2R-trans)-2-(3,4-dihydroxyphenyl)-3,4-dihydro-2H-1-benzopyran-3,5,7-triol T=30°C; pH=7.0; 240 h; Product distribution; Further Variations:Reagents;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 4 p. 415 - 422