1-甲氧基-4-[(三氟甲基)磺酰基]苯合成路线 （共 11 条）
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
copper(I) oxide in N,N-dimethyl-formamide T=50°C; 18 h; Inert atmosphere;
参考文献
Cullen, Steven C.; Shekhar, Shashank; Nere, Nandkishor K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12194 - 12201
反应条件
copper(I) oxide in N,N-dimethyl-formamide T=50°C; 18 h; Inert atmosphere;
参考文献
Cullen, Steven C.; Shekhar, Shashank; Nere, Nandkishor K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12194 - 12201
反应条件
in diethyl ether T=-78°C;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2727 - 2729
参考文献
Shein,S.M. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1966 , vol. 36, # 12 p. 2141 - 2147,2135 - 2141
反应条件
triethylamine in 2,2,2-trifluoroethanol 22 h; Photolysis;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 8 p. 1232 - 1236
反应条件
palladium diacetate in water; N,N-dimethyl-formamide T=20°C; 22 h;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 5 p. 928 - 931
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in dimethyl sulfoxide T=80°C; Stille coupling reaction; P=2068.59 Torr; 72 h; 2: With trifluoroacetic acid in dichloromethane T=23°C; 0.5 h;
参考文献
Yun, Weiya; Li, Shiming; Wang, Bingbing; Chen, Li
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 175 - 177
反应条件
triethylamine in 2,2,2-trifluoroethanol 22 h; Photolysis;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 8 p. 1232 - 1236
反应条件
triethylamine in 2,2,2-trifluoroethanol 28 h; Photolysis;
参考文献
De Carolis, Marco; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1232 - 1236
