N,N-二甲基-3-硝基苄胺合成路线 （共 14 条）
反应条件
triethylamine in N-methyl-acetamide; water
参考文献
Chugai Seiyaku Kabushiki Kaisha
Patent: US6534546 B1, 2003 ;
反应条件
in tetrahydrofuran; toluene 2 h; Heating;
参考文献
ABBOTT LABORATORIES; BA-MAUNG, Nwe Y.; CLARK, Richard F.; ERICKSON, Scott A.; FIDANZE, Steve D.; KAWAI, Megumi; MANTEI, Robert A.; SHEPPARD, George S.; SORENSON, Bryan K.; WANG, Gary T.
Patent: WO2011/53476 A1, 2011 ;
Location in patent: Page/Page column 162 ;
WO 2011/053476 A1
反应条件
1: With sulfuric acid 2: Alkaline conditions;
参考文献
Cedilote, Miall; Cleary, Thomas Patrick; Zhang, Pingsheng
Patent: US2007/255057 A1, 2007 ;
Location in patent: Page/Page column 1; 4 ;
反应条件
1: With tert-butyl methyl ether; nitric acid in tetrahydrofuran T=0°C; 2: With sulfuric acid in dichloromethane T=0°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Zhang, Pingsheng; Cedilote, Miall; Cleary, Thomas P.; Pierce, Michael E.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8659 - 8664
反应条件
formic acid T=185 - 190°C; 6 h;
参考文献
Sharma; Kaur, Sukhvir
Journal of the Indian Chemical Society, 2007 , vol. 84, # 6 p. 612 - 614
参考文献
Goss; Ingold; Wilson
Journal of the Chemical Society, 1926 , p. 2458
参考文献
Goss; Ingold; Wilson
Journal of the Chemical Society, 1926 , p. 2458
参考文献
Hoefnagel, A. J.; Vos, R. H. de; Wepster, B. M.
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 1 p. 22 - 28
反应条件
titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 10 h, 2.) 25 deg C, 10 h; Yield given. Multistep reaction;
参考文献
Bhattacharyya, Sukanta
Journal of Organic Chemistry, 1995 , vol. 60, # 15 p. 4928 - 4929
参考文献
Sommelet; Guioth
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1922 , vol. 174, p. 689
Full Text Show Details
Goss; Ingold; Wilson
Journal of the Chemical Society, 1926 , p. 2458
