O,O,O-三甲基巯基磷酸酯合成路线 （共 58 条）
反应条件
sulfur trioxide in dichloromethane
T=-95°C;
参考文献
Ando, Fumio; Koketsu, Jugo; Ishii, Yoshio
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3495 - 3499
反应条件
boron trifluoride-methanol
1) 0 deg C, 1h, 2) RT, overnight;
参考文献
Ryu, Seungmin; Jackson, John A.; Thompson, Charles M.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 4999 - 5002
反应条件
Lawesson's reagent in benzene
13.5 h; Heating; Yields of byproduct given;
参考文献
Zabirov, N. G.; Cherkasov, R. A.; Khalikov, I. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 12 p. 2673 - 2677,2365 - 2368
反应条件
boron trifluoride-methanol
1) 0 deg C, 1h, 2) RT, overnight;
参考文献
Ryu, Seungmin; Jackson, John A.; Thompson, Charles M.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 4999 - 5002
反应条件
phosphorous acid trimethyl ester
Heating;
参考文献
Friedrich, Klaus; Gallmeier, Hans-Joachim
Tetrahedron Letters, 1981 , vol. 22, # 31 p. 2971 - 2972
反应条件
in dichloromethane
2 h; Heating;
参考文献
Sato, Ryu; Murata, Toshitaka; Chida, Shin-ichi; Ogawa, Satoshi
Chemistry Letters, 1993 , # 8 p. 1325 - 1328
反应条件
[2,2']bipyridinyl; copper(II) bis(trifluoromethanesulfonate)
T=25°C; Kinetics; Further Variations:Reagents;
参考文献
Neverov, Alexei A.; Brown, R. Stan
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 15 p. 2245 - 2248
反应条件
in acetonitrile
T=25°C;
参考文献
Ponomarov, Oleksandr; Laws, Andrew P.; Hanusek, Jiri
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8868 - 8876
反应条件
in 1,2-dichloro-ethane
T=20°C; 0.0833333 h;
参考文献
Kamer; Roelen; Van den Elst; Van der Marel; Van Boom
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6757 - 6760
反应条件
sulfur trioxide in dichloromethane
T=-78°C; other trialkyl phosphite,trialkyl phosphine, trialkyl arsines, trialkoxyarsines, var. molar ratio and temperatures; Product distribution;
参考文献
Ando, Fumio; Koketsu, Jugo; Ishii, Yoshio
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3495 - 3499
