O,O,O-三甲基巯基磷酸酯合成路线 (共 58 条)
反应条件
potassium hydroxide in water
0.25 h;
参考文献
Das, Sushanta K.; Balasubrahmanyam, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 254 - 256
参考文献
Iyer; Phillips; Egan; Regan; Beaucage
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4693 - 4699
反应条件
phosphorous acid trimethyl ester
T=100 - 105°C; 30 h; Yield given;
参考文献
Ayral-Kaloustain, Semiramis; Agosta, William C.
Synthetic Communications, 1981 , vol. 11, # 12 p. 1011 - 1016
反应条件
thiophosphoryl trichloride
参考文献
Pistschimuka
Chemische Berichte, 1908 , vol. 41, p. 3855
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1418
Chem. Zentralbl., 1913 , vol. 84, # I p. 1581
反应条件
in diethyl ether
react. of a soln. in ether with a suspension of NaOCH3 in ether;;
参考文献
Gmelin Handbook: P: MVol.C, 260, page 594 - 596
Full Text Show Details
Simon, A.; Schulze, G.
Z. Anorg. Chem., 1939 , vol. 242, p. 313 - 368
参考文献
Middleton,W.J.; Sharkey,W.H.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1384 - 1390
参考文献
Middleton,W.J.; Sharkey,W.H.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1384 - 1390
反应条件
P=1E-05 - 0.001 Torr; Ambient temperatureproton affinity, Δ G, Δ H; Thermodynamic dataEquilibrium constant;
参考文献
Hodges, Ronald V.; McDonnell, T. J.; Beauchamp, J. L.
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1327 - 1332
反应条件
1,1-dioxo-3H-1,2-benzodithiol-3-one in acetonitrile
further reagents (3H-1,2-benzodithiol-3-one 1-oxide, 3H-1,2-benzothiol-3-one); Product distributionMechanism;
参考文献
Stawinski, Jacek; Thelin, Mats
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5169 - 5175
反应条件
in diethyl ether; Petroleum ether
Ambient temperaturesolvents: diethylether, accetonitrile; MechanismProduct distribution;
参考文献
Mikolajczyk, Marian; Kielbasinski, Piotr; Basinski, Wlodzimierz
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 899 - 908