O,O,O-三甲基巯基磷酸酯合成路线 (共 58 条)
反应条件
water
T=25°C; KineticsProduct distribution; Further Variations:Reagents;
参考文献
Kevill, Dennis N.; Carver, Jeffrey S.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 2040 - 2043
反应条件
in acetonitrile
T=30°C; 0.0833333 h; Kinetics;
参考文献
Hanusek, Jiri; Russell, Mark A.; Laws, Andrew P.; Page, Michael I.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 417 - 419
参考文献
Pistschimuka
Chemische Berichte, 1908 , vol. 41, p. 3855
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1418
Chem. Zentralbl., 1913 , vol. 84, # I p. 1581
反应条件
perchloric acid; (S)-{2-[2-(4-tert-butyl)oxazolinyl]phenyl-C1,N}(trifluoromethylpyridine)(aqua)-palladium(II) triflate
T=25°C; pH=10.8; aq. buffer; Kinetics; Reagent/catalystpH-value;
参考文献
Lu, Zhong-Lin; Yang, Xiao-Sheng; Guo, Zhi-Fo; Wang, Rui-Yao
Journal of Coordination Chemistry, 2010 , vol. 63, # 14-16 p. 2659 - 2672
反应条件
perchloric acid; (S)-{2-[2-(4-tert-butyl)oxazolinyl]phenyl-C1,N}(trifluoromethylpyridine)(aqua)-palladium(II) triflate
T=25°C; pH=10.8; aq. buffer; Kinetics;
参考文献
Lu, Zhong-Lin; Yang, Xiao-Sheng; Guo, Zhi-Fo; Wang, Rui-Yao
Journal of Coordination Chemistry, 2010 , vol. 63, # 14-16 p. 2659 - 2672
反应条件
T=60°C; other temperature; Rate constant;
参考文献
Lebedev, N. N.; Kiryushatova, T. V.; Savel'yanov, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 9 p. 2141 - 2144,1913 - 1915
参考文献
Walling; Rabinowitz
Journal of the American Chemical Society, 1959 , vol. 81, p. 1243,1247
参考文献
Miyamoto, Toru; Yamamoto, Izuru
Agricultural and Biological Chemistry, 1981 , vol. 45, # 9 p. 1991 - 1998
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
through polysulfide species, thiirane and its oxides; instead of N-ethylmaleimide: acetonitrile; var. time, temp.; Product distributionMechanism;
参考文献
Swinson, Joel; Field, Lamar; Heimer, Norman E.; Stone, Michael P.; Wazer, John R. Van
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 39 - 52
反应条件
trichlorophosphate
T=20°C; multistep reaction; varying of molar ratio of components; time taken in the addition of alcohol; consumption time of reactants; alcoholysis of PSCl3 (estimation of rel. rates); Product distribution;
参考文献
Avetisov, Ya. K.; Zatsepin, V. M.; Zaripova, V. Sh.; Bondarenko, G. M.; Savchenko, B. M.; Kalachik, B. S.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 10 p. 2304 - 2310,2059 - 2065