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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
15226-74-1
合成路线
（共 158 条）
15226-74-1
+
765-30-0
环丙胺
→
反应条件
88229-13-4
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
15226-74-1
→
反应条件
1235569-11-5
+
79655-71-3
反应条件
1: dicobalt octacarbonyl; N,N,N'-trimethyl-N'-allylthiourea; phenylacetylene With 1,1,3,3-tetramethyl-2-thiourea in toluene Pauson-Khand reaction; 0.0833333 h; Inert atmosphere; 2: carbon monoxide in toluene T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 48 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359
15226-74-1
→
反应条件
612-71-5
1,3,5-三苯基苯
+
1235569-11-5
+
1165-53-3
+
79655-71-3
反应条件
1: dicobalt octacarbonyl; N,N,N'-trimethyl-N'-allylthiourea; phenylacetylene With 1,1,3,3-tetramethyl-2-thiourea in toluene Pauson-Khand reaction; 0.0833333 h; Inert atmosphere; 2: carbon monoxide in toluene T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 24 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359
15226-74-1
+
628-71-7
1-庚炔
→
反应条件
89506-33-2
反应条件
1: dicobalt octacarbonyl; 1-n-heptyne; N,N,N'-trimethyl-N'-allylthiourea With 1,1,3,3-tetramethyl-2-thiourea in toluene Pauson-Khand reaction; 0.0833333 h; Inert atmosphere; 2: carbon monoxide in toluene T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 24 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359
15226-74-1
+
106192-73-8
→
反应条件
97398-02-2
+
89787-00-8
反应条件
byproducts: CoBr2, CO;
参考文献
Kroeckert, Bernd; Paetzold, Peter
Chemische Berichte, 1987 , vol. 120, p. 631 - 634
15226-74-1
+
20469-65-2
+
6148-64-7
→
反应条件
97025-16-6
反应条件
1H-imidazole; palladium diacetate; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; magnesium chloride in tetrahydrofuran T=90°C; 0.5 h; Microwave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 25 p. 3525 - 3528
15226-74-1
+
992-94-9
+
7647-19-0
→
反应条件
21329-73-7
+
21329-74-8
+
21329-72-6
反应条件
below room temp., then warming to room temp;;
参考文献
Gondal, S. K.; MacDiarmid, A. G.; McDowell, M. V.
Inorganic and Nuclear Chemistry Letters, 1969 , vol. 5, p. 351 - 354
Full Text View citing articles Show Details
Gmelin Handbook: Co: Org.Verb.1, 1.1.4.3.2, page 77 - 81
110-91-8
+
626-55-1
+
15226-74-1
→
反应条件
492-85-3
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
15226-74-1
+
38395-67-4
→
反应条件
5635-16-5
反应条件
calcium hydroxide powder; carbon monoxide; methyl iodide in methanol; water 20°C, 20 h.;
参考文献
Miura, Masahiro; Okuro, Kazumi; Hattori, Ayako; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 73 - 76
110-91-8
+
15226-74-1
+
1122-91-4
→
反应条件
58287-80-2
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
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