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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-溴-2-萘酚
合成路线
（共 198 条）
15231-91-1
6-溴-2-萘酚
→
反应条件
78119-82-1
6-羟基-2-萘甲醛
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78 - -64°C; 0.416667 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=-78 - 20°C; 1.33333 h; 3: With citric acid in tetrahydrofuran pH=5; 0.5 h;
参考文献
Olsen, Helle Birk; kaarsholm, Niels C.; Madsen, Peter; Ostergaard, Soren; Ludvigsen, Svend; Jakobsen, Palle; Petersen, Anders Klarskov; Steensgaard, Dorte Bjerre
Patent: US2003/229120 A1, 2003 ;
Location in patent: Page 52 ;
2591-86-8
+
15231-91-1
6-溴-2-萘酚
→
反应条件
78119-82-1
6-羟基-2-萘甲醛
反应条件
1: 6-bromo-2-hydroxy-naphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.25 h; 2: 1-piperidinecarboxaldehyde in tetrahydrofuran; hexane T=-78 - 20°C; 0.25 h;
参考文献
Gabbutt, Christopher D.; Heron, B. Mark; Kilner, Colin; Kolla, Suresh B.
Dyes and Pigments, 2012 , vol. 94, # 2 p. 175 - 182
15231-91-1
6-溴-2-萘酚
→
反应条件
1353573-04-2
+
26628-47-7
反应条件
1: sulfuric acid / 4 h / 120 - 125 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / 22 h / Reflux; Inert atmosphere View Scheme
参考文献
Azizian, Farid; Field, Amanda J.; Heron, B. Mark; Kilner, Colin
Chemical Communications, 2012 , vol. 48, # 5 p. 750 - 752
15231-91-1
6-溴-2-萘酚
→
反应条件
1353573-05-3
+
26628-47-7
反应条件
1: sulfuric acid / 4 h / 120 - 125 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / 22 h / Reflux; Inert atmosphere View Scheme
参考文献
Azizian, Farid; Field, Amanda J.; Heron, B. Mark; Kilner, Colin
Chemical Communications, 2012 , vol. 48, # 5 p. 750 - 752
15231-91-1
6-溴-2-萘酚
→
反应条件
65283-60-5
+
13185-00-7
反应条件
air; (NO+)Ru(II)-salen in toluene T=25°C; Arylation; 24 h; Irradiation; Product distribution; Further Variations:various amount of catalyst;
参考文献
Somei, Hidenori; Asano, Yasuaki; Yoshida, Tomokazu; Takizawa, Shinobu; Yamataka, Hiroshi; Sasai, Hiroaki
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1841 - 1844
15231-91-1
6-溴-2-萘酚
→
反应条件
13185-00-7
反应条件
oxygen; N-ketopinidene-L-tert-leucine oxovanadium(IV) in tetrachloromethane T=40 - 45°C; 192 h;
参考文献
Barhate, Nivrutti B.; Chen, Chien-Tien
Organic Letters, 2002 , vol. 4, # 15 p. 2529 - 2532
15231-91-1
6-溴-2-萘酚
+
30889-48-6
→
反应条件
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
15231-91-1
6-溴-2-萘酚
+
1150311-11-7
→
反应条件
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 48 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
15231-91-1
6-溴-2-萘酚
+
1150311-12-8
→
反应条件
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 48 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
15231-91-1
6-溴-2-萘酚
→
反应条件
52927-22-7
反应条件
CuCN in N,N-dimethyl-formamide T=160 - 170°C; 3 h;
参考文献
Aoyama; Okutome; NakayamaT.; Yaegashi; Matsui; Nunomura; Kurumi; Sakurai; Fujii
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 4 p. 1458 - 1471
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