二乙基(2-甲基苯基)膦酸酯合成路线 （共 21 条）
反应条件
N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=70°C; 34 h; in sealed tube;
参考文献
Petrakis, Konstantinos S.; Nagabhushan, Tattanahalli L.
Journal of the American Chemical Society, 1987 , vol. 109, # 9 p. 2831 - 2833
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) T=90°C; 30 h;
参考文献
Hirao, Toshikazu; Masunaga, Toshio; Yamada, Naoto; Ohshiro, Yoshiki; Agawa, Toshio
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 3 p. 909 - 913
反应条件
Mn(OAc)3•2H2O in acetic acid T=60°C; 7 h;
参考文献
Xu, Wei; Zou, Jian-Ping; Zhang, Wei
Tetrahedron Letters, 2010 , vol. 51, # 19 p. 2639 - 2643
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
反应条件
nickel dichloride T=180°C; 0.5 h;
参考文献
Grabiak, Raymond C.; Miles, James A.; Schwenzer, Gretchen M.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 197 - 202
反应条件
NiII chloride hexahydrate; potassium bromide T=185 - 190°C; Arbuzov reaction; 36 h; Inert atmosphere;
参考文献
Yang, Guoqiang; Shen, Chaoren; Zhang, Liang; Zhang, Wanbin
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5032 - 5035
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium (II) trifluoroacetate; p-benozquinone in methanol T=120°C; 0.333333 h; Microwave irradiation;
参考文献
Andaloussi, Mounir; Lindh, Jonas; Saevmarker, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 13069 - 13074
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; N-ethyl-N,N-diisopropylamine; zinc in N,N-dimethyl-formamide T=100°C; 36 h; Inert atmosphere;
参考文献
Shen, Chaoren; Yang, Guoqiang; Zhang, Wanbin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 17 p. 3500 - 3505
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in toluene T=100°C; 19 h;
参考文献
Hirao, Toshikazu; Masunaga, Toshio; Yamada, Naoto; Ohshiro, Yoshiki; Agawa, Toshio
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 3 p. 909 - 913
反应条件
1: pyridine / dichloromethane / Inert atmosphere 2: 1,1'-bis-(diphenylphosphino)ferrocene; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; N-ethyl-N,N-diisopropylamine; zinc / N,N-dimethyl-formamide / 36 h / 100 °C / Inert atmosphere View Scheme
参考文献
Shen, Chaoren; Yang, Guoqiang; Zhang, Wanbin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 17 p. 3500 - 3505
