1: With potassium carbonate in 1,4-dioxane Wittig reaction; 24 h; Heating; 2: With dichloro bis(acetonitrile) palladium(II) in dichloromethane T=20°C; 24 h; Further stages.;
n-butyllithium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane Yield given;
参考文献
Marples, Brian A.; Saint, Christopher G.; Traynor, John R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 567 - 574
1: (ethyl)-triphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=20°C; Wittig Olefination; 0.0833333 h; 2: pentanal in tetrahydrofuran Wittig Olefination;
参考文献
Baccolini, Graziano; Delpivo, Camilla; Micheletti, Gabriele
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1291 - 1302
