2,3,4,5,6-五氟苯甲酮合成路线 (共 15 条)
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.5 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1373 - 1381
反应条件
1: 1-bromo-2,3,4,5,6-pentafluorobenzene With n-butyllithium in diethyl ether T=-75°C; Inert atmosphere; 2: benzoic acid methyl ester in diethyl ether T=-75°C; Inert atmosphere;
参考文献
Inorganic Chemistry, , vol. 51, # 5 p. 2893 - 2901
反应条件
in diethyl ether reaction at 15°C, 15 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in o-xylene T=150°C; 16 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 4 p. 1665 - 1669
反应条件
hydrogenchloride in diethyl ether 1.) -78 deg C, 35 min; 2.) -78 deg C;
参考文献
Journal of Fluorine Chemistry, , vol. 19, p. 43 - 54
反应条件
chromium(VI) oxide; acetic acid
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: (i) Mg, (ii) /BRN= 471223/ 2: CrO3, AcOH View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: (i) Mg, (ii) /BRN= 471223/ 2: CrO3, AcOH View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
aluminium trichloride
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 38, # 11 p. 2493 - 2497,2409 - 2412
反应条件
(i) Mg, (ii) /BRN= 471389/; Multistep reaction;
参考文献
Journal of the Chemical Society, , p. 808 - 817