3-脱氧-D-甘油-D-乳-2-吡喃壬酮糖酸合成路线 （共 4 条）
反应条件
ozone in dimethylsulfide; water T=20°C; 1 h;
参考文献
Crich, David; Navuluri, Chandrasekhar
Organic Letters, 2011 , vol. 13, # 23 p. 6288 - 6291
反应条件
1: tetrahydrofuran; toluene / 3.25 h / -60 - 0 °C / Reflux; Inert atmosphere 2: N-bromosuccinmide; silver nitrate / acetone / 2 h / 20 °C / Inert atmosphere; Darkness 3: acetic acid / water / 60 h / 40 °C 4: ozone / dimethylsulfide; water / 1 h / 20 °C View Scheme
参考文献
Crich, David; Navuluri, Chandrasekhar
Organic Letters, 2011 , vol. 13, # 23 p. 6288 - 6291
反应条件
1: sodium tetrahydroborate / methanol / 2 h / -15 °C / Inert atmosphere 2: N-bromosuccinmide; silver nitrate / acetone / 2 h / 20 °C / Inert atmosphere; Darkness 3: acetic acid / water / 60 h / 40 °C 4: ozone / dimethylsulfide; water / 1 h / 20 °C View Scheme
参考文献
Crich, David; Navuluri, Chandrasekhar
Organic Letters, 2011 , vol. 13, # 23 p. 6288 - 6291
反应条件
1: tetrahydrofuran; toluene / -40 - 0 °C / Inert atmosphere 2: sodium tetrahydroborate / methanol / 2 h / -15 °C / Inert atmosphere 3: N-bromosuccinmide; silver nitrate / acetone / 2 h / 20 °C / Inert atmosphere; Darkness 4: acetic acid / water / 60 h / 40 °C 5: ozone / dimethylsulfide; water / 1 h / 20 °C View Scheme
参考文献
Crich, David; Navuluri, Chandrasekhar
Organic Letters, 2011 , vol. 13, # 23 p. 6288 - 6291
