您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
153865-87-3
合成路线
（共 9 条）
110-00-9
呋喃
+
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=100°C; 2 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
271-89-6
氧茚
+
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; N,N-dimethyl-formamide T=100°C; 1 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
108-38-3
间二甲苯
+
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; N,N-dimethyl-formamide T=100°C; 1 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
100-66-3
苯甲醚
+
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; N,N-dimethyl-formamide T=100°C; 1 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
1: diethyl ether; dichloromethane / 18 h / 0 °C 2: tetrabutyl ammonium fluoride; tris-(dibenzylideneacetone)dipalladium(0); thiophene / tetrahydrofuran; N,N-dimethyl-formamide; water / 1 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
429-41-4
四丁基氟化铵
+
108-88-3
甲苯
+
153865-87-3
→
反应条件
717-00-0
1-苄基嘧啶-2,4-二酮
反应条件
tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran; water; N,N-dimethyl-formamide T=100°C; 6 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
153865-87-3
+
71-43-2
苯
→
反应条件
61686-79-1
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; N,N-dimethyl-formamide T=100°C; 1 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
153865-87-3
→
反应条件
61686-79-1
反应条件
1: diethyl ether; dichloromethane / 18 h / 0 °C 2: toluene; tetrabutyl ammonium fluoride; tris-(dibenzylideneacetone)dipalladium(0) / tetrahydrofuran; N,N-dimethyl-formamide; water / 1 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
153865-87-3
→
反应条件
61686-79-1
反应条件
1: diethyl ether; dichloromethane / 18 h / 0 °C 2: palladium diacetate; caesium carbonate; 2,2,2-trimethylacetic acid / N,N-dimethyl-formamide / 2 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
