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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
154197-00-9
合成路线
（共 22 条）
6952-59-6
间溴苯腈
+
31268-20-9
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
71426-20-5
+
154197-00-9
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
696-62-8
4-碘苯甲醚
+
100-47-0
苯甲腈
→
反应条件
58743-77-4
4-甲氧基-4’-氰基联苯
+
125610-78-8
4-甲氧基-2-氰基联苯
+
154197-00-9
反应条件
bathophenanthroline; sodium t-butanolate T=182°C; 6 h; Inert atmosphere;
参考文献
Zhao, Huaiqing; Shen, Jie; Guo, Juanjuan; Ye, Ruijuan; Zeng, Huaqiang
Chemical Communications, 2013 , vol. 49, # 23 p. 2323 - 2325
104-92-7
4-溴苯甲醚
+
150255-96-2
3-氰基苯硼酸
→
反应条件
154197-00-9
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran; water Suzuki Coupling; 2 h; Reflux;
参考文献
Bang, Joon Seok; Kim, Young Jin; Song, Jiho; Yoo, Jong-Sun; Lee, Seul; Lee, Mi Ji; Min, Hyeyoung; Hwang, Kwang Woo; Min, Kyung Hoon
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 17 p. 5262 - 5268
873-62-1
3-氰基苯酚
→
反应条件
154197-00-9
反应条件
1: Et3N 2: methanol / 1 h / Irradiation; photolysis of 4-methoxyphenyl aryl alkylphosphonates, solvent effect View Scheme
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
150-76-5
4-甲氧基苯酚
→
反应条件
154197-00-9
反应条件
1: Et3N / diethyl ether 2: Et3N 3: methanol / 1 h / Irradiation; photolysis of 4-methoxyphenyl aryl alkylphosphonates, solvent effect View Scheme
参考文献
Nakamura, Mitsunobu; Sawasaki, Kouiti; Okamoto, Yoshiki; Takamuku, Setsuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 141 - 146
1235553-97-5
→
反应条件
154197-00-9
反应条件
1: potassium acetate / tert-butyl alcohol / 2 h / 90 °C / Inert atmosphere 2: potassium phosphate / tert-butyl alcohol / 2 h / 90 °C / Inert atmosphere View Scheme
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
49584-07-8
→
反应条件
154197-00-9
反应条件
1: potassium acetate / tert-butyl alcohol / 2 h / 90 °C / Inert atmosphere 2: potassium phosphate / tert-butyl alcohol / 2 h / 90 °C / Inert atmosphere View Scheme
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
104-92-7
4-溴苯甲醚
+
100-47-0
苯甲腈
→
反应条件
58743-77-4
4-甲氧基-4’-氰基联苯
+
125610-78-8
4-甲氧基-2-氰基联苯
+
154197-00-9
反应条件
HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5)(1+)*Cl(1-)=(HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5))Cl; potassium tert-butylate T=20 - 100°C; 24 h; Schlenk techniqueInert atmosphereGreen chemistry; Overall yield = 65 percentSpectr.; regioselective reaction;
参考文献
Ghosh, Debalina; Lee, Jhen-Yi; Liu, Chian-Yu; Chiang, Yen-Hsin; Lee, Hon Man
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 406 - 410
104-94-9
对甲氧基苯胺
+
100-47-0
苯甲腈
→
反应条件
154197-00-9
反应条件
hydrogenchloride; sodium hydroxide; sodium nitrite 1.) 0 deg C, 2.) 8 h; Multistep reaction;
参考文献
Nakamura, Mitsunobu; Sawasaki, Kouiti; Okamoto, Yoshiki; Takamuku, Setsuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 141 - 146
154197-00-9
→
反应条件
725-05-3
4’-甲氧基联苯-3-羧酸
反应条件
1: With potassium hydroxide in ethanol; water T=120°C; 0.5 h; Microwave irradiation; 2: With hydrogenchloride in water
参考文献
Bang, Joon Seok; Kim, Young Jin; Song, Jiho; Yoo, Jong-Sun; Lee, Seul; Lee, Mi Ji; Min, Hyeyoung; Hwang, Kwang Woo; Min, Kyung Hoon
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 17 p. 5262 - 5268
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