alkali hydroxide in water addn. of aq. alkali hydroxide to an aq. soln. of equival. amts. of Cu(ClO4)2 and 2-amino-benzoic acid at 20°C;; ppt.; drying at 20°C in air;;
alkali hydroxide in water addn. of aq. alkali hydroxide to an aq. soln. of equival. amts. of CuCl2 and 2-amino-benzoic acid at 20°C;; ppt.; drying at 20°C in air;;
in water ppt.; washing with H2O and ethanol (several times); drying at 130°C in vac.;;
参考文献
Hill, A. G.; Curran, C.
Journal of Physical Chemistry, 1960 , vol. 64, p. 1519 - 1522
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Gmelin Handbook: Cu: MVol.B4, 98, page 1650 - 1652
NaOH; acid in water free acid ligand was dissolved in dilute aq. NaOH, adjusted with diluteacid to pH 6-7; prepd. soln. was filterted and added to aq. soln. of metal acetate; filtration, washing, air drying; elem. anal.;
参考文献
Albanese, N. F.; Haendler, H. M.
Polyhedron, 1983 , vol. 2, p. 1131 - 1140
