4-(3-丁烯-1-基)溴苯合成路线 （共 10 条）
反应条件
in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Molander, Gary A.; Sandrock, Deidre L.
Journal of the American Chemical Society, 2008 , vol. 130, # 47 p. 15792 - 15793
反应条件
in tetrahydrofuran T=0 - 20°C; 29 h;
参考文献
OSTA BIOTECHNOLOGIES; The Sir Mortimer B. Davis - Jewish General Hospital; QUEEN'S UNIVERSITY AT KINGSTON
Patent: WO2008/151437 A1, 2008 ;
Location in patent: Page/Page column 72-73 ;
反应条件
1: in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: With phosphonic acid diethyl ester in tetrahydrofuran Inert atmosphere;
参考文献
Li, Ying; Hu, Yuan-Yuan; Zhang, Song-Lin
Chemical Communications, 2013 , vol. 49, # 90 p. 10635 - 10637
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 889
Bulletin de la Societe Chimique de France, , vol. <4> 45, p. 80,84
反应条件
(i) Mg, (ii) /BRN= 605308/; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 33, # 3 p. 972 - 977
参考文献
Chemistry - A European Journal, , vol. 12, # 3 p. 721 - 726
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Peterson,P.E. et al.
Journal of Organic Chemistry, 1968 , vol. 33, # 3 p. 972 - 977
反应条件
1: 4-(3-butenyl)-1-bromobenzene With iodine; magnesium in tetrahydrofuran T=0 - 20°C; 2.01667 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran 0.0833333 h; Inert atmosphereReflux;
参考文献
Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2013 , vol. 49, # 95 p. 11230 - 11232
反应条件
1: dimethylformamide / Heating 2: NaOH / aq. ethanol / Heating View Scheme
参考文献
Peterson,P.E. et al.
Journal of Organic Chemistry, 1968 , vol. 33, # 3 p. 972 - 977
反应条件
1: 4-(3-butenyl)-1-bromobenzene With iodine; magnesium in tetrahydrofuran T=0 - 20°C; 2.01667 h; Inert atmosphere; 2: N,N-dimethyl-formamide in tetrahydrofuran; diethyl ether T=0 - 20°C; 1.03333 h; Inert atmosphere;
参考文献
Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2013 , vol. 49, # 95 p. 11230 - 11232
