4-(3-丁烯-1-基)苯甲酸合成路线 （共 6 条）
反应条件
1: 4-(3-butenyl)-1-bromobenzene With iodine; magnesium in tetrahydrofuran T=0 - 20°C; 2.01667 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran 0.0833333 h; Inert atmosphereReflux;
参考文献
Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2013 , vol. 49, # 95 p. 11230 - 11232
反应条件
1: (i) Mg, (ii) /BRN= 605308/ 2: dimethylformamide / Heating 3: NaOH / aq. ethanol / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 33, # 3 p. 972 - 977
反应条件
sodium hydroxide in ethanol Heating;
参考文献
Journal of Organic Chemistry, , vol. 33, # 3 p. 972 - 977
反应条件
1: dimethylformamide / Heating 2: NaOH / aq. ethanol / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 33, # 3 p. 972 - 977
反应条件
1: 1) Mg / 1) THF, 80 deg C, 2 h, 2) reflux, 15 h 2: 1) Mg, ethyliodine / 1) THF, a) reflux, 3 h, b) stirred overnight, 2) THF, 5-15 deg C, 30 min View Scheme
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 199, p. 345 - 378
反应条件
magnesium; ethyl iodide 1) THF, a) reflux, 3 h, b) stirred overnight, 2) THF, 5-15 deg C, 30 min; Multistep reaction;
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 199, p. 345 - 378
