N,N-二甲基苯硫代甲酰胺合成路线 (共 49 条)
反应条件
Yield given. Yields of byproduct given;
参考文献
Jen, Kwan-Yue; Cava, Michael P.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2001 - 2004
反应条件
(i) Py, (ii) P2S5; Multistep reaction;
参考文献
Voss,J.; Walter,W.
Justus Liebigs Annalen der Chemie, 1968 , vol. 716, p. 209 - 211
参考文献
Kienle, Marcel; Unsinn, Andreas; Knochel, Paul
Angewandte Chemie - International Edition, 2010 , vol. 49, # 28 p. 4751 - 4754
参考文献
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
hydrogenchloride; N-Nitrosomorpholine; potassium iodide in dichloromethane; water T=22°C; 50 h;
参考文献
Joergensen, K. A.; Ghattas, A.-B.A.G.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 9 p. 1163 - 1168
反应条件
sodium tetrahydroborate in acetonitrile 26 h; Heating;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 8 p. 505 - 512
反应条件
1: CH2Cl2 / 12 h / Ambient temperature 2: 5 percent / Et3N / CH2Cl2 / Ambient temperature View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 71, p. 197 - 206
参考文献
Journal of Organic Chemistry, , vol. 16, p. 131,133
反应条件
sodium tetrahydroborate in acetonitrile 26 h; Heating;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 8 p. 505 - 512
反应条件
hydrogenchloride; dimethylsulfide borane complex 1.) toluene, reflux, 30 min, 2.) reflux, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 756 - 784