2-(苯甲酰基)-4,5-二氯哒嗪-3-酮合成路线 （共 20 条）
反应条件
zinc(II) chloride in acetonitrile 7 h; Heating;
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Kim, Ho-Kyun; Cho, Su-Dong; Kang, Young-Jin; Park, Ki Hun; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthetic Communications, 2005 , vol. 35, # 3 p. 371 - 378
反应条件
in tetrahydrofuran 34 h; Heating;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
Amberlite(R) IRA-67 in acetonitrile T=20°C; 0.75 h;
参考文献
Kim, Jeum-Jong; Park, Young-Dae; Kim, Ho-Kyun; Cho, Su-Dong; Kim, Ju-Kyeong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthetic Communications, 2005 , vol. 35, # 5 p. 731 - 738
反应条件
1: 2-benzoyl-4,5-dichloropyridazin-3(2H)-one With hydrazine hydrate in tetrahydrofuran
T=20°C; 0.166667 h;
2: 4,5-Dichloro-2-(4-methyl-benzoyl)-2H-pyridazin-3-one in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Chung, Hyun-A; Kweon, Deok-Heon; Cho, Su-Dong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2003 , # 4 p. 560 - 564
反应条件
in tetrahydrofuran
T=150°C; P=10336 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Kim, Bo Ram; Sung, Gi Hyeon; Lee, Sang-Gyeong; Yoon, Yong Jin
Tetrahedron, 2013 , vol. 69, # 15 p. 3234 - 3237
反应条件
in tetrahydrofuran
T=18°C; 12 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
1: 2-benzoyl-4,5-dichloropyridazin-3(2H)-one With hydrazine hydrate in tetrahydrofuran
T=20°C; 0.166667 h;
2: 4,5-dichloro-2-(4-chloro-benzoyl)-2H-pyridazin-3-one in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Chung, Hyun-A; Kweon, Deok-Heon; Cho, Su-Dong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2003 , # 4 p. 560 - 564
反应条件
in dichloromethane
T=22°C; 0.166667 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
in toluene
2 h; RefluxGreen chemistry;
参考文献
Sung, Gi Hyeon; Lee, In-Hye; Kim, Bo Ram; Shin, Dong-Soo; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Tetrahedron, 2013 , vol. 69, # 17 p. 3530 - 3535
反应条件
1.1: NH2NH2*H2O / tetrahydrofuran / 0.17 h / 20 °C
1.2: tetrahydrofuran / 0.17 h / 20 °C
2.1: polyphosphoric acid / 3.5 h / 130 °C
View Scheme
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Chung, Hyun-A; Kweon, Deok-Heon; Cho, Su-Dong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2003 , # 4 p. 560 - 564
