2-甲基-1,5-戊二胺合成路线 （共 17 条）
反应条件
HZSM-5(280) zeolite in water T=300°C; Cyclization;
参考文献
Radha Rani; Srinivas; Kulkarni; Raghavan
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 3 p. 286 - 290
反应条件
ammonia; oxygen; V2O5/hydrotalcite in water T=425°C; 1.5 - 4 h; Product distribution / selectivity;
参考文献
EP961770 B1, ;
Page/Page column 5-6 ;
反应条件
ammonia; oxygen; V2O5/Al2O3-SiO2 in water T=391°C; 0.9 - 2.9 h; Product distribution / selectivity;
参考文献
REILLY INDUSTRIES, INC.
Patent: EP961770 B1, 2003 ;
Location in patent: Page/Page column 8 ;
反应条件
ammonia; oxygen; V2O5/Al2O3-SiO2 T=400°C; 0.9 - 2.9 h; Product distribution / selectivity;
参考文献
REILLY INDUSTRIES, INC.
Patent: EP961770 B1, 2003 ;
Location in patent: Page/Page column 8 ;
参考文献
Monsanto Compamy
Patent: US5189205 A1, 1993 ;
反应条件
methanesulfonic acid; triethylamine in toluene 63.5 h; Reflux;
参考文献
DESIGNER MOLECULES, INC.; DERSHEM, Stephen
Patent: WO2010/19832 A2, 2010 ;
Location in patent: Page/Page column 64 ;
反应条件
1: With 5 wt ruthenium/carbon; aluminium in water
T=150°C; 2.5 h;
2: With hydrogenchloride in dichloromethane
参考文献
Gaedda, Thomas M.; Yu, Xiao-Yan; Miyazawa, Akira
Tetrahedron, 2010 , vol. 66, # 6 p. 1249 - 1253
