2-(3-甲氧基苯基)环己酮合成路线 (共 13 条)
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene 20 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
n-butyllithium in tetrahydrofuran; hexane; cyclohexanone
参考文献
US6284755 B1, ;
US 6284755 B1
反应条件
in anhydrous xylene; 2-chlorocyclohexan-1-one
参考文献
Nachtsheim, Corina M.; Frahm, August W.
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 187 - 197
反应条件
1.1: 32 percent / tetrahydrofuran / 2 h / -78 °C 2.1: EtONa / ethanol / 1 h / 20 °C 2.2: 46 percent / aq. HCl / ethanol / 0 °C View Scheme
参考文献
Synthesis, , # 6 p. 845 - 848
反应条件
1.1: 32 percent / tetrahydrofuran / 2 h / -78 °C 2.1: EtONa / ethanol / 1 h / 20 °C 2.2: 46 percent / aq. HCl / ethanol / 0 °C View Scheme
参考文献
Synthesis, , # 6 p. 845 - 848
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 17, p. 581,588
反应条件
sodium amide in tetrahydrofuran
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1047 - 1050
反应条件
1.1: copper(l) iodide / tetrahydrofuran / 0.5 h / 20 °C 1.2: 8 h / 20 °C 2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 10 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 19 p. 7134 - 7137
反应条件
ammonium cerium(IV) nitrate; pentacarbonylmanganese tetrafluoroborate; sodium acetate
参考文献
Journal of Organometallic Chemistry, , vol. 258, # 2 p. C41 - C44