苄基-Alpha-D-吡喃甘露糖苷合成路线 (共 13 条)
反应条件
acetyl chloride T=20 - 50°C; 16.5 h; Inert atmosphere;
参考文献
Zunk, Matthew; Kiefel, Milton J.
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1296 - 1299
反应条件
acetyl chloride T=50°C; 2 h;
参考文献
Li, Tiehai; Wen, Liuqing; Williams, Adriel; Wu, Baolin; Li, Lei; Qu, Jingyao; Meisner, Jeffrey; Xiao, Zhongying; Fang, Junqiang; Wang, Peng George
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 1139 - 1147
反应条件
sodium methylate in methanol T=20°C; 3 h; Inert atmosphere;
参考文献
Polakova, Monika; Roslund, Mattias U.; Ekholm, Filip S.; Saloranta, Tiina; Leino, Reko
European Journal of Organic Chemistry, 2009 , # 6 p. 870 - 888
反应条件
acetyl chloride 50 deg C for 1.5 h then room temperature for 24 h;
参考文献
Bashyal, Bharat P.; Fleet, George W. J.; Gough, Max J.; Smith, Paul W.
Tetrahedron, 1987 , vol. 43, # 13 p. 3083 - 3094
参考文献
Tetrahedron Letters, , vol. 32, # 43 p. 6089 - 6092
反应条件
hydrogenchloride; acetyl chloride
参考文献
Dziewiszek, Krzysztof; Banaszek, Anna; Zamojski, Aleksander
Tetrahedron Letters, 1987 , vol. 28, # 14 p. 1569 - 1572
反应条件
hydrogenchloride 1.) 60 deg C, 4 h, 2.) room temp., overnight;
参考文献
Winnik; Carver; Krepinsky
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2701 - 2707
反应条件
gold(III) chloride in acetonitrile 5.5 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 21 p. 8417 - 8420
反应条件
methanol 2 h; Reflux;
参考文献
Journal of Organic Chemistry, , vol. 79, # 3 p. 1100 - 1110
反应条件
1: 28 percent / formic acid / 0.25 h 2: 51 percent / n-Bu4NHSO4, aq NaOH / CH2Cl2 / 20 h / Heating View Scheme
参考文献
Winnik; Carver; Krepinsky
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2701 - 2707