1-(硫代苯甲酰基)哌啶合成路线 （共 35 条）
反应条件
2: hydrogen sulfide / ethanol 3: sodium hydroxide 4: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 18 p. 5070 - 5076
反应条件
1: 76 percent / benzene / standing overnight 2: 95 percent / H2S (gas) / ethanol / 1.) -60 - 50 deg C, 13 hrs., 2.) -15 deg C, overnight View Scheme
参考文献
Chen, Shoujun; Sun, Lijun; Koya, Keizo; Tatsuta, Noriaki; Xia, Zhiqiang; Korbut, Timothy; Du, Zhenjian; Wu, Jim; Liang, Guiqing; Jiang, Jun; Ono, Mitsunori; Zhou, Dan; Sonderfan, Andrew
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 18 p. 5070 - 5076
反应条件
dinitrogen tetraoxide in tetrachloromethane; acetonitrile T=0°C; 0.166667 h;
参考文献
Kim, Hyung Jin; Kim, Yong Hae
Synthesis, 1986 , # 11 p. 970 - 972
反应条件
2: 95 percent / pyridine / 16 h / Ambient temperature View Scheme
参考文献
Liebigs Annalen der Chemie, , p. 179 - 182
反应条件
1: tetrahydrofuran / Ambient temperature 2: 77 percent Chromat. / NaBH3CN / methanol; H2O; acetic acid / 2 h View Scheme
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
2: 99 percent / pyridine / 16 h / Ambient temperature View Scheme
参考文献
Santus, Maria
Liebigs Annalen der Chemie, 1988 , p. 179 - 182
反应条件
toluene-4-sulfonic acid; sulfur
Willgerodt-Kindler reaction; 4 h; Reflux;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
tetraphosphorus decasulfide in 1,4-dioxane
2 h; Ambient temperature;
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
sulfur in benzene
T=80°C; 0.75 h;
参考文献
Aly, Moustafa F.; Grigg, Ronald
Tetrahedron, 1988 , vol. 44, # 23 p. 7271 - 7282
反应条件
triethylamine in benzene
Thioacylation;
参考文献
Doszczak; Rachon
Chemical Communications, 2000 , # 21 p. 2093 - 2094
