反式-1,2-二氯乙烯合成路线 (共 182 条)
反应条件
T=24°C; unter Stickstoff; Kinetics;
参考文献
Swedlund; Robertson
Journal of the Chemical Society, 1947 , p. 632
反应条件
triethylamine; NiCl2((PPh3)P)2 in N,N-dimethyl-formamide T=120°C; 7 h;
参考文献
Shulyupin, Mstilsav O.; Chirkov, Evgeniy A.; Kazankova, Marina A.; Beletskaya, Irina P.
Synlett, 2005 , # 4 art. no. G46004ST, p. 658 - 660
反应条件
1: chloro-diphenylphosphine With potassium in 1,4-dioxane 10 h; Heating; 2: trans-1,2-dichloroethylene in 1,4-dioxane T=20°C; 10 h; Further stages.;
参考文献
Brunner, Henri; Muschiol, Manfred; Zabel, Manfred
Synthesis, 2008 , # 3 p. 405 - 408
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; 56 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; 56 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; 56 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; 56 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; 56 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
oxygen; chlorine in neat (no solvent) T=30°C; P=1050.08 Torr; Irradiation; MechanismRate constantProduct distribution;
参考文献
Griesbaum, Karl; Hayes, Michael P.; Werli, Vera
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1366 - 1370
反应条件
methyl 2,2,3,3,3-pentafluoropropyl ether; chlorine T=24.84°C; P=7598.26 Torr; PhotolysisSynthetic airGas phase; Kinetics;
参考文献
Morozov; Nielsen; Morozova; Vasiliev; Loukhovitskaya
Russian Chemical Bulletin, 2010 , vol. 59, # 4 p. 754 - 760