3-(4-甲氧基苯基)丙酸甲酯合成路线 (共 45 条)
反应条件
1: thionyl chloride / 0 - 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 23 p. 6058 - 6061
反应条件
methanol; TEA in tetrahydrofuran 4 h; Heating;
参考文献
Tetrahedron Letters, , vol. 42, # 26 p. 4309 - 4312
反应条件
iodine; potassium carbonate 80 h; Heating;
参考文献
Mori, Naoshi; Togo, Hideo
Tetrahedron, 2005 , vol. 61, # 24 p. 5915 - 5925
反应条件
ammonium cerium (IV) nitrate T=20°C; 4 h; Inert atmosphere;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1472 - 1479
反应条件
1: potassium carbonate / acetonitrile / 50 °C 2: nickel dichloride; triphenylphosphine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane / tetrahydrofuran / 16 h / 50 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 4 p. 1529 - 1541
反应条件
1: potassium carbonate / acetonitrile / 50 °C 2: nickel dichloride; triphenylphosphine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane / tetrahydrofuran / 16 h / 50 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 4 p. 1529 - 1541
反应条件
methanol Esterification;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 14 p. 1519 - 1522
反应条件
anhydrous tetramethylammonium chloride; sodium hydride 1.) hexane, 25 deg C, 30 min; 50 deg C, 2 h, 2.) methyl ethyl ketone, 50 - 60 deg C, 30 min, 3.) RT, 6 h;
参考文献
Fatope, Majekodunmi O.; Adeniyl, Adebayo E.
Synthetic Communications, 1985 , vol. 15, # 4 p. 307 - 310
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2 in tetrahydrofuran T=120°C; 36 h; Schlenk techniqueInert atmosphere; Catalytic behavior; Reagent/catalyst;
参考文献
Organometallics, , vol. 31, # 23 p. 8200 - 8207
参考文献
Journal of the Chemical Society, , p. 1412
Journal of the Chemical Society, , p. 607,609