2,4-双(氯甲基)三甲基苯合成路线 （共 18 条）
反应条件
zinc(II) chloride T=20°C; 0.166667 h;
参考文献
Shimizu, Tomoe; Hida, Katsuhiko; Yamato, Takehiko
Journal of Chemical Research, 2009 , # 7 p. 443 - 447
反应条件
hydrogenchloride T=65°C; Einleiten von HCl;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 55, p. 1000,1003
反应条件
hydrogenchloride 2 h; Heating; Title compound not separated from byproducts.;
参考文献
Russian Journal of General Chemistry, , vol. 77, # 4 p. 611 - 619
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 6, p. 1025,1033
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 6, p. 1025,1033
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 204, p. 1826
反应条件
T=65°C; Einleiten von HCl;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 55, p. 1000,1003
反应条件
1: bis-diphenylphosphine With n-butyllithium in tetrahydrofuran; hexane T=-40 - 0°C; Metallation; 2: 1,3-bis(chloromethyl)-2,4,6-trimethylbenzene in tetrahydrofuran; hexane T=20°C; Condensation; Heating; Further stages.;
参考文献
Cohen, Revital; Van Der Boom, Milko E.; Shimon, Linda J. W.; Rozenberg, Haim; Milstein, David
Journal of the American Chemical Society, 2000 , vol. 122, # 32 p. 7723 - 7734
反应条件
1: toluene; zinc; aq. NaOH solution 2: aqueous formaldehyde; concentrated aqueous hydrochloric acid View Scheme
参考文献
Aitken et al.
Journal of the Chemical Society, 1950 , p. 331,334
反应条件
1: silver acetate; glacial acetic acid 2: aqueous KOH View Scheme
参考文献
Nauta; Dienske
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 1000,1003
反应条件
sodium hydroxide; toluene; zinc
参考文献
Rudenko, A. P.; Korovina, N. S.; Aver'yanov, S. F.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 8 p. 1077 - 1083
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 8 p. 1184 - 1190
