in neat (no solvent) addn. of P4S10 to CH3OSn(CH2CH2CH2CH3)3; stirring at 15°C for 2 h;; evacuation at 0.03 mmHg at 40°C for 1 h; molecular-film distn. with temp. in the thermoelement spiral 140-150°C (0.02 mmHg); elem. anal.;;
参考文献
Nizamov, I. S.; Kuznetsov, V. A.; Batyeva, E. S.; Al'fonsov, V. A.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1992 , vol. 62, p. 1366 - 1367
Zhurnal Obshchei Khimii, 1992 , vol. 62, p. 1665 - 1666
in 1,4-dioxane; water PhCOCHOHPh and P4S10 reacted in dioxane under reflux for 2 h, NiCl2*6H2O added, mixture reacted in dioxane/water under reflux; elem. anal.;
参考文献
Kajitani, Masatsugu; Yoshida, Yasuki; Akiyama, Takeo; Sugimori, Akira
Nippon Kagaku Kaishi (Journal of the Chemical Society of Japan), 1985 , vol. 60, p. 433 - 437
