5,5'-二溴-2,2'-联吡啶合成路线 （共 20 条）
反应条件
hexamethyl-distannane; tetrakis(triphenylphosphine) palladium(0) in benzene 65 h; Heating;
参考文献
Bruce, James I.; Chambron, Jean-Claude; Koelle, Philipp; Sauvage, Jean-Pierre
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1226 - 1231
反应条件
1: 3-bromopyridinetrifluoroborate With lithium diisopropyl amide in diethyl ether T=-78°C; Inert atmosphere; 2: 3-bromo-pyridine in diethyl ether T=-78°C; Inert atmosphere; 3: With water
参考文献
Dhau, Jaspreet S.; Singh, Amritpal; Kasetti, Yoganjaneyulu; Bhatia, Sonam; Bharatam, Parsad V.; Brandao, Paula; Felix, Vitor; Singh, Kamal N.
Tetrahedron, 2013 , vol. 69, # 48 p. 10284 - 10291
反应条件
n-butyllithium in toluene T=0°C; 0.0833333 h;
参考文献
US2006/30714 A1, ;
Page/Page column 6 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 20 h; Inert atmosphereReflux;
参考文献
Collin, Jean-Paul; Durola, Fabien; Lux, Jacques; Sauvage, Jean-Pierre
New Journal of Chemistry, 2010 , vol. 34, # 1 p. 34 - 43
反应条件
tetrakis(triphenylphosphine) palladium(0) in xylene T=110°C; Stille coupling reaction; 32 h;
参考文献
Schwab, Peter F.H.; Fleischer, Frank; Michl, Josef
Journal of Organic Chemistry, 2002 , vol. 67, # 2 p. 443 - 449
反应条件
2,6-bis(trimethylstannyl)-pyridine; tetrakis(triphenylphosphine) palladium(0) in toluene 60 h; Heating;
参考文献
Lehmann, Uwe; Henze, Oliver; Schlueter, A. Dieter
Chemistry - A European Journal, 1999 , vol. 5, # 3 p. 854 - 859
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; Stille coupling; 5 h; Inert atmosphere;
参考文献
Krompiec; Ignasiak; Stanek; Filapek; Gebarowska; Penczek
Polish Journal of Chemistry, 2009 , vol. 83, # 2 p. 245 - 262
反应条件
tetrakis(triphenylphosphine) palladium(0); 1,1,1,2,2,2-hexabutyl-distannane in toluene T=125°C; Sonogashira coupling; 72 h;
参考文献
Ayme, Jean-Francois; Beves, Jonathon E.; Leigh, David A.; McBurney, Roy T.; Rissanen, Kari; Schultz, David
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9488 - 9497
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; Stille coupling; 3 h; Inert atmosphere;
参考文献
Polish Journal of Chemistry, , vol. 83, # 2 p. 245 - 262
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 60 h; Heating;
参考文献
Lehmann, Uwe; Henze, Oliver; Schlueter, A. Dieter
Chemistry - A European Journal, 1999 , vol. 5, # 3 p. 854 - 859
