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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-(邻甲苯)苯并噻唑
合成路线
（共 24 条）
89-93-0
2-甲基苯甲基胺
+
615-43-0
2-碘苯胺
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
95-16-9
苯并噻唑
+
16419-60-6
2-甲基苯硼酸
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
potassium phosphate; 1,10-phenanthroline; copper diacetate; palladium diacetate in dimethyl sulfoxide T=100°C; 24 h;
参考文献
Ranjit, Sadananda; Liu, Xiaogang
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1105 - 1108
95-16-9
苯并噻唑
+
89-95-2
2-甲基苯甲醇
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
95-16-9
苯并噻唑
+
615-37-2
2-碘代甲苯
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=85°C; 36 h; Inert atmosphere;
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672
95-16-9
苯并噻唑
+
95-46-5
邻溴甲苯
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=85°C; 36 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
529-20-4
2-甲基苯甲醛
+
137-07-5
2-氨基苯硫醇
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water 2.5 h; Reflux;
参考文献
Azarifar, Davood; Khosravi, Kaveh; Najminejad, Zohreh; Soleimani, Khadijeh
Heterocycles, 2010 , vol. 81, # 12 p. 2855 - 2863
95-16-9
苯并噻唑
+
95-49-8
2-氯甲苯
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
[Fe(II)(C5H5)(C5H4PPh2)]; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=140°C; 40 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
615-43-0
2-碘苯胺
+
529-20-4
2-甲基苯甲醛
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993
95-16-9
苯并噻唑
+
529-20-4
2-甲基苯甲醛
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
dipotassium peroxodisulfate in water; dimethyl sulfoxide T=100°C; 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
305858-45-1
→
反应条件
15903-58-9
2-(邻甲苯)苯并噻唑
反应条件
1: With copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide T=80°C; 15 h; Inert atmosphere; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; 8 h;
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
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