3-环己基-3-氧代丙酸乙酯合成路线 （共 21 条）
反应条件
niobium pentachloride in dichloromethane T=27°C; 3.5 h;
参考文献
Yadav; Subba Reddy; Eeshwaraiah; Reddy
Tetrahedron, 2005 , vol. 61, # 4 p. 875 - 878
反应条件
1: With 1-methyl-1H-imidazole in toluene T=-45°C; 0.166667 h; 2: With titanium tetrachloride; N-ethyl-N,N-diisopropylamine in toluene T=-45°C; 0.5 h;
参考文献
Misaki, Tomonori; Nagase, Ryohei; Matsumoto, Kunshi; Tanabe, Yoo
Journal of the American Chemical Society, 2005 , vol. 127, # 9 p. 2854 - 2855
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-70 - -65°C; 0.5 h;
参考文献
WO2004/22560 A1, ;
Page 33-34 ;
WO 2004/022560 A1
反应条件
hydrogen; Lindlar's catalyst in methanol
参考文献
Zhurnal Organicheskoi Khimii, , vol. 3, p. 1213 - 1220,1175 - 1180
反应条件
1: benzene-1,4-diol / benzene / 140 - 150 °C 2: H2 / Pd-CaCO3 / methanol View Scheme
参考文献
Zhurnal Organicheskoi Khimii, , vol. 3, p. 1213 - 1220,1175 - 1180
反应条件
diethyl ether Einleiten von Ammoniak in eine aether. Loesung des Reaktionsprodukts;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 2197,2200
反应条件
1: DMAP / tetrahydrofuran / 24 h / Ambient temperature 2: 1.) TMSCl; 2.) DBU / 1.) acetonitrile, room t.; 2.) 0 degC, 0.5 h, room t., 17 h View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9323 - 9326
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 241, p. 602
反应条件
Reaktion ueber mehrere Stufen;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1286
反应条件
sodium hydroxide 1. 20 h, room temp.; 2. pyrolysis at 110 deg C; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 43 - 47
