4-甲氧苯基2,6-二-O-苄基-β-D-吡喃葡萄糖苷合成路线 （共 8 条）
反应条件
water; trifluoroacetic acid in dichloromethane T=0°C; 2 h;
参考文献
Nakahara, Yoshiaki; Iijima, Hiroyuki; Ogawa, Tomoya
Tetrahedron Letters, 1994 , vol. 35, # 20 p. 3321 - 3324
反应条件
1: 91.3 percent / NaH / dimethylformamide / 5 h 2: 92 percent / acetic acid; H2O / 2 h / 80 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 11 p. 2386 - 2394
反应条件
1: 64 percent / CSA / dimethylformamide / 8 h 2: 91.3 percent / NaH / dimethylformamide / 5 h 3: 92 percent / acetic acid; H2O / 2 h / 80 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 11 p. 2386 - 2394
反应条件
1: 100 percent / NaOMe / methanol / 1 h 2: 64 percent / CSA / dimethylformamide / 8 h 3: 91.3 percent / NaH / dimethylformamide / 5 h 4: 92 percent / acetic acid; H2O / 2 h / 80 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 11 p. 2386 - 2394
反应条件
1: 90 percent / TfOH; 4 Angstroem molecular sieves / CH2Cl2 / 1 h 2: 100 percent / NaOMe / methanol 3: 79 percent / CSA / dimethylformamide 4: 77 percent / NaH / dimethylformamide / 5 h 5: 73 percent / aq. AcOH / 2 h View Scheme
参考文献
Synlett, , # 9 SPEC. ISS. p. 1315 - 1318
反应条件
1: 90 percent / TfOH; 4 Angstroem molecular sieves / CH2Cl2 / 1 h 2: 100 percent / NaOMe / methanol 3: 79 percent / CSA / dimethylformamide 4: 77 percent / NaH / dimethylformamide / 5 h 5: 73 percent / aq. AcOH / 2 h View Scheme
参考文献
Synlett, , # 9 SPEC. ISS. p. 1315 - 1318
反应条件
1: 98 percent / NaH / tetrahydrofuran / 20 h / 60 °C 2: 95 percent / 80percent CF3CO2H, water / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 20 p. 3321 - 3324
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in acetonitrile T=-40°C; 1 h; Molecular sieveInert atmosphere;
参考文献
Carbohydrate Research, , vol. 361, p. 91 - 99,9
