4-甲氧苯基-3,4-O-异亚丙基-β-D-吡喃半乳糖苷合成路线 （共 8 条）
反应条件
camphor-10-sulfonic acid in N,N-dimethyl-formamide
参考文献
Belot, Frederic; Otter, Albin; Fukuda, Minoru; Hindsgaul, Ole
Synlett, 2003 , # 9 SPEC. ISS. p. 1315 - 1318
反应条件
iodine; toluene-4-sulfonic acid T=45°C; 0.333333 h;
参考文献
Zhao, Guilong; Zhang, Yan; Wang, Jianwu
Collection of Czechoslovak Chemical Communications, 2007 , vol. 72, # 9 p. 1214 - 1218
反应条件
(1S)-10-camphorsulfonic acid T=20°C; 48 h;
参考文献
Carbohydrate Research, , vol. 341, # 10 p. 1630 - 1644
反应条件
1: 100 percent / NaOMe / methanol / 1 h 2: 64 percent / CSA / dimethylformamide / 8 h View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 11 p. 2386 - 2394
反应条件
1: 90 percent / TfOH; 4 Angstroem molecular sieves / CH2Cl2 / 1 h 2: 100 percent / NaOMe / methanol 3: 79 percent / CSA / dimethylformamide View Scheme
参考文献
Synlett, , # 9 SPEC. ISS. p. 1315 - 1318
反应条件
1: 90 percent / TfOH; 4 Angstroem molecular sieves / CH2Cl2 / 1 h 2: 100 percent / NaOMe / methanol 3: 79 percent / CSA / dimethylformamide View Scheme
参考文献
Synlett, , # 9 SPEC. ISS. p. 1315 - 1318
反应条件
sodium hydride in tetrahydrofuran T=60°C; 20 h;
参考文献
Nakahara, Yoshiaki; Iijima, Hiroyuki; Ogawa, Tomoya
Tetrahedron Letters, 1994 , vol. 35, # 20 p. 3321 - 3324
反应条件
1: 91.3 percent / NaH / dimethylformamide / 5 h 2: 92 percent / acetic acid; H2O / 2 h / 80 °C View Scheme
参考文献
Nakahara, Yoshiaki; Iijima, Hiroyuki; Ogawa, Tomoya
Tetrahedron Letters, 1994 , vol. 35, # 20 p. 3321 - 3324
