反式-1-苯基-1-戊烯合成路线 (共 108 条)
反应条件
dirhodium(II) tetrakis(perfluorobutyrate) in benzene
Heating;
参考文献
Doyle, Michael P.; High, Kenneth G.; Oon, Su-Min; Osborn, Antonio K.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3049 - 3052
反应条件
[CuOTf][(Sa,R,R)-phosphoramidite derivative]2 in tetrahydrofuran; hexane
T=-60°C; 18 h; Product distribution; Further Variations:CatalystsSolventsTemperatures;
参考文献
Van Zijl, Anthoni W.; Arnold, Leggy A.; Minnaard, Adriaan J.; Feringa, Ben L.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 4 p. 413 - 420
反应条件
in diethyl ether; hexane
T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu; Nagase, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 673 - 678
反应条件
in tetrahydrofuran
T=25°C; 2 h; other aldehydes; Product distribution;
参考文献
Jeganathan, Suruliappa; Tsukamoto, Masamitsu; Schlosser, Manfred
Synthesis, 1990 , # 2 p. 109 - 111
反应条件
in diethyl ether; hexane
T=0°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu; Nagase, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 673 - 678
反应条件
water
8 h; Heating; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barsegyan, S. K.; Gasparyan, G. Ts.; Ovakimyan, M. Zh.; Indzhikyan, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 5 p. 977 - 983,859 - 864
反应条件
triethyl phosphite in tetrahydrofuran; dichloromethane
T=20°C; 0.166667 h; Product distribution; Further Variations:TemperaturesSolvents;
参考文献
Tonder, Janne E; Hosseini, Masood; Ahrenst, Alex B; Tanner, David
Organic and biomolecular chemistry, 2004 , vol. 2, # 10 p. 1447 - 1455
反应条件
triethyl phosphite in tetrahydrofuran; dichloromethane
T=20°C; 0.166667 h; Product distribution; Further Variations:TemperaturesSolvents;
参考文献
Tonder, Janne E; Hosseini, Masood; Ahrenst, Alex B; Tanner, David
Organic and biomolecular chemistry, 2004 , vol. 2, # 10 p. 1447 - 1455
反应条件
lithium diisopropyl amide; methyl iodide
1) THF, 0 deg C, 1 h, 2) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schwan, Adrian L.; Wilson, David A.
Tetrahedron Letters, 1992 , vol. 33, # 40 p. 5897 - 5900
反应条件
rhodium (II) acetate in toluene
T=102°C; Product distribution;
参考文献
Doyle, Michael P.; High, Kenneth G.; Oon, Su-Min; Osborn, Antonio K.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3049 - 3052