二环己烷并-18-冠醚-6合成路线 （共 9 条）
反应条件
potassium hydroxide; tetrabutylammomium bromide in toluene T=90°C; 15 h;
参考文献
Kusov, S. Z.; Lubenets, E. G.; Kobrin, V. S.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.2 p. 1234 - 1236
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1485 - 1488
反应条件
hydrogen; 4-amino-benzoic acid in isopropyl alcohol T=82°C; catalytic hydrogenation;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 6 p. 1309 - 1313,1163 - 1166
反应条件
potassium hydroxide; DCH18C6 T=80°C; 10 h;
参考文献
Yakshin, V. V.; Zhukova, N. G.; Tsarenko, N. A.; Laskorin, B. N.
Doklady Chemistry, 1983 , vol. 273, p. 436 - 438
Dokl. Akad. Nauk SSSR Ser. Khim., 1983 , vol. 273, # 6 p. 1398 - 1400
反应条件
1: 10 percent / tetrabutylammonium bromide 2: 35.4 percent / 50percent aq. KOH, tetrabutylammonium bromide / toluene / 15 h / 90 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 7.2 p. 1234 - 1236
Zhurnal Organicheskoi Khimii, , vol. 29, # 7 p. 1485 - 1488
反应条件
hydrogen; Rh on carbon in water; isopropyl alcohol T=100°C; P=37503 Torr; oth. catalysts, oth. solvents, var. H2 pressure, rate and selectivity of reaction; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, # 3 p. 543 - 547
Zhurnal Organicheskoi Khimii, , vol. 24, # 3 p. 607 - 612
反应条件
potassium hydroxide; DCH18C6
参考文献
Yakshin, V. V.; Zhukova, N. G.; Tsarenko, N. A.; Laskorin, B. N.
Doklady Chemistry, 1983 , vol. 273, p. 436 - 438
Dokl. Akad. Nauk SSSR Ser. Khim., 1983 , vol. 273, # 6 p. 1398 - 1400
反应条件
potassium hydroxide; DCH18C6
参考文献
Yakshin, V. V.; Zhukova, N. G.; Tsarenko, N. A.; Laskorin, B. N.
Doklady Chemistry, 1983 , vol. 273, p. 436 - 438
Dokl. Akad. Nauk SSSR Ser. Khim., 1983 , vol. 273, # 6 p. 1398 - 1400
反应条件
in acetone detd. by NMR;
参考文献
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, , vol. 27, # 3 p. 150 - 151
反应条件
in methanol
standing at 20°C to solvent evapn.; residue dilution with acetone/hexane, soln. partial evapn., upper layer decanting, residue washing with hot hexane, crystn. from ethyl acetate;
参考文献
Ganin
Russian Journal of General Chemistry, 1998 , vol. 68, # 1 p. 8 - 9
