water; ammonium chloride
in situ nucleophilic acylation of alkyl and phenyl isocyanates by t-BuLi, sec-BuLi, n-BuLi. Temp.: -110 to -135 deg C.; Product distribution;
参考文献
Seyferth, Dietmar; Hui, Richard C.
Tetrahedron Letters, 1984 , vol. 25, # 46 p. 5251 - 5254
in benzene
under N2, stirred under reflux for 2 h; taken to dryness, filtered, washed with Et2O, dried under vac.; elem. anal.;
参考文献
Hills, Adrian; Hughes, David L.; Leigh, G. Geffery; Prieto-Alcon, Rafael
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1993 , # 23 p. 3609 - 3618
