1-(2-羟基-4,6-二甲基苯基)乙酮合成路线 （共 33 条）
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
T=140°C; 72 h; Yield given. Further byproducts given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
T=140°C; 72 h; Further byproducts given. Yields of byproduct given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
7 h; Heating; Further byproducts given;
参考文献
Marquet, Jorge; Moreno-Manas, Marcial; Pacheco, Pedro; Prat, Maria; Katritzky, Alan R.; Brycki, Bogumil
Tetrahedron, 1990 , vol. 46, # 15 p. 5333 - 5346
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
7 h; Heating; Further byproducts given;
参考文献
Marquet, Jorge; Moreno-Manas, Marcial; Pacheco, Pedro; Prat, Maria; Katritzky, Alan R.; Brycki, Bogumil
Tetrahedron, 1990 , vol. 46, # 15 p. 5333 - 5346
反应条件
carbon disulfide; aluminium trichloride
参考文献
Fuson et al.
Journal of the American Chemical Society, 1943 , vol. 65, p. 1028
反应条件
in neat (no solvent)
byproducts: C6H3(CH3)2OH, C6H2(CH3)2COCH3OCOCH3, C6H3(CH3)2OCOCH3; mixed, refluxed for 24 h, cooled to room temp., pptd.; elem. anal., XRD;
参考文献
Arias, Jose Luis; Cabrera, Armando; Sharma, Pankaj; Rosas, Noe; Garcia, Jose Luis; Hernandez
Inorganica Chimica Acta, 2000 , vol. 310, # 2 p. 261 - 264
反应条件
pyridine
24 h; Heating;
参考文献
Bravo, Pierfrancesco; Resnati, Giuseppe; Ticozzi, Calimero; Arnone, Alberto; Cavicchio, Giancarlo
Gazzetta Chimica Italiana, 1986 , vol. 116, # 9 p. 501 - 510
反应条件
potassium carbonate; caesium carbonate in dimethyl sulfoxide
Heating;
参考文献
Shrout, David P.; Lightner, David A.
Synthetic Communications, 1990 , vol. 20, # 13 p. 2075 - 2080
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
17 h; Heating; Yield given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
pyridine
24 h; Heating;
参考文献
Bravo, Pierfrancesco; Resnati, Giuseppe; Ticozzi, Calimero; Arnone, Alberto; Cavicchio, Giancarlo
Gazzetta Chimica Italiana, 1986 , vol. 116, # 9 p. 501 - 510
