1-(2-羟基-4,6-二甲基苯基)乙酮合成路线 （共 33 条）
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
17 h; Heating; Yield given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
17 h; Heating; Yield given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
pyridine
24 h; Heating;
参考文献
Bravo, Pierfrancesco; Resnati, Giuseppe; Ticozzi, Calimero; Arnone, Alberto; Cavicchio, Giancarlo
Gazzetta Chimica Italiana, 1986 , vol. 116, # 9 p. 501 - 510
反应条件
pyridine
14 h; Heating;
参考文献
Bravo, Pierfrancesco; Resnati, Giuseppe; Ticozzi, Calimero; Arnone, Alberto; Cavicchio, Giancarlo
Gazzetta Chimica Italiana, 1986 , vol. 116, # 9 p. 501 - 510
参考文献
Kindler et al.
Archiv der Pharmazie (Weinheim, Germany), 1954 , vol. 287, p. 210,223
反应条件
carbon disulfide; aluminium trichloride
参考文献
v.Auwers; Borsche
Chemische Berichte, 1915 , vol. 48, p. 1707
Full Text Show Details
v.Auwers
Chemische Berichte, 1915 , vol. 48, p. 92
反应条件
palladium on barium sulfate
参考文献
Lacey,R.N.
Journal of the Chemical Society, 1960 , p. 1625 - 1633
反应条件
pyridine hydrochloride
参考文献
Royer,R. et al.
Bulletin de la Societe Chimique de France, 1973 , p. 611 - 615
参考文献
Wittig
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 179
反应条件
1: 90 percent / KH
2: 1.) CeCl3 / 1.) THF, 1 h room temp., 1.5 h -78 deg C, 2.) THF, 4 h -78 deg C
3: 97.7 percent / 20percent aq. HCl / methanol / 0.17 h / 80 deg C bath temperature
View Scheme
参考文献
Nagasawa, Kazuo; Kanbara, Hajime; Matsushita, Kazuya; Ito, Keiichi
Tetrahedron Letters, 1985 , vol. 26, # 52 p. 6477 - 6480
