phosphorus pentachloride in trichlorophosphate T=120°C; 12 h;
参考文献
Karaman, Rafik; Blasko, Andrei; Almarsson, Oern; Arasasingham, Ramesh; Bruice, Thomas C.
Journal of the American Chemical Society, 1992 , vol. 114, # 12 p. 4889 - 4898
1: With isopropylmagnesium chloride in tetrahydrofuran T=20°C; 0.5 h; 2: With sulfur dioxide in tetrahydrofuran T=-40°C; 0.5 h; 3: With sulfuryl dichloride in tetrahydrofuran T=-40 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 68, # 21 p. 8274 - 8276
1: With hydrogenchloride in water T=30°C; Sandmeyer reaction; 2: With sodium nitrite in water T=-5 - 0°C; Sandmeyer reaction; 0.916667 h; 3: With thionyl chloride; water; copper(l) chloride T=-5 - 0°C; Sandmeyer reaction; 2.83333 h;
参考文献
Hogan, Philip J.; Cox, Brian G.
Organic Process Research and Development, 2009 , vol. 13, # 5 p. 875 - 879
