2,4,6-三甲基苯磺酰肼合成路线 （共 6 条）
反应条件
perchloric acid in 1,4-dioxane; water T=0°C; 7.58333 h;
参考文献
WO2003/72553 A1, ;
Page/Page column 135 ;
反应条件
hydrazine in dichloromethane 0.25 h;
参考文献
Antimicrobial Agents and Chemotherapy, , vol. 46, # 8 p. 2450 - 2457
反应条件
1: Br2 2: (i) CF3SO3Ag, (ii) /BRN= 969212/ View Scheme
参考文献
Effenberger,F.; Huthmacher,K.
Chemische Berichte, 1976 , vol. 109, p. 2315 - 2326
反应条件
sulfuryl dichloride; triethylamine
1.) CH2Cl2, 0 deg C; 2.) CH2Cl2, pyridine, 0 deg C; Yield given. Multistep reaction;
参考文献
Back, Thomas G.; Collins, Scott; Krishna, M. Vijaya
Canadian Journal of Chemistry, 1987 , vol. 65, p. 38 - 42
反应条件
in methanol
1.) 50 deg, 2.) room temperature;
参考文献
Bertz, Steven H.; Dabbagh, Gary
Journal of Organic Chemistry, 1983 , vol. 48, # 1 p. 116 - 119
反应条件
in tetrahydrofuran
T=0°C; 16 h;
参考文献
Bryant, Michael W.; Smith, Robin A. J.; Wong, Lisa
Australian Journal of Chemistry, 1982 , vol. 35, # 12 p. 2529 - 2540
