3,5-二叔丁基-4-羟基苯甲醛合成路线 （共 132 条）
反应条件
pyridine; potassium hydroxide; dihydrogen peroxide in water
0.666667 h; Heating;
参考文献
Selassie, Cynthia D.; Verma, Rajeshwar P.; Kapur, Sanjay; Shusterman, Alan J.; Hansch, Corwin
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 6 p. 1112 - 1117
反应条件
1: LiAlH4; diethyl ether
2: acetyl chloride
View Scheme
参考文献
Coppinger; Campbell
Journal of the American Chemical Society, 1953 , vol. 75, p. 734
参考文献
Monash University
Patent: US6232314 B1, 2001 ;
反应条件
in n-heptane
Condensation; 1 h; Heating;
参考文献
Masere, Jonathan
Patent: US2012/313036 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
1: heptane / 1 h / Heating
2: 55.7 g / heptane / 1 h / 80 °C
3: 83.7 percent / Ac2O / toluene / 1 h / Heating
View Scheme
参考文献
Nesvadba, Peter
Synthetic Communications, 2000 , vol. 30, # 15 p. 2825 - 2832
反应条件
1: 59 percent / tetrahydrofuran; diethyl ether; cyclohexane
2: 81 percent / trimethylsilyl chloride / CH2Cl2 / 3 h
View Scheme
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
1: 90 percent / 0.5 h / 180 °C
2: 67.3 percent / 35percent HCl / H2O; dioxane / 1 h / Heating
View Scheme
参考文献
Bannikov, G. F.; Nikiforov, G. A.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 6 p. 1289 - 1291
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 6 p. 1408 - 1410
反应条件
in benzene
T=21°C; relative equilibrium constants; other 2,6-di-tert-butylphenols and bicyclic phenols;
参考文献
Jackson, Richard A.; Hosseini, Kamran Mousavi
Journal of the Chemical Society, Chemical Communications, 1992 , # 13 p. 967 - 968
反应条件
air; chloroacetic acid in xylene
1.5 h; Heating;
参考文献
Semeikin, A. S.; Koifman, O. I.; Berezin, B. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 6 p. 629 - 632
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 6 p. 798 - 801
反应条件
pyridine-4-carbaldehyde in propionic acid
3 h; Heating;
参考文献
Milgrom; Hill; Dempsey
Tetrahedron, 1994 , vol. 50, # 47 p. 13477 - 13484
