[(环己基氧基)甲基]苯合成路线 （共 80 条）
反应条件
1: chloro-trimethyl-silane / 2 h / 23 °C / Inert atmosphere
2: 4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 - 23 °C / Inert atmosphere
3: dichloromethane / 0.08 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
in dichloromethane-d2
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
tetrachloromethane; bis(acetylacetonate)oxovanadium; triethylamine
T=175°C; 10 h; Inert atmosphereAutoclave;
参考文献
Khusnutdinov; Bayguzina; Gallyamova; Dzhemilev
Petroleum Chemistry, 2012 , vol. 52, # 4 p. 261 - 266
反应条件
in dichloromethane-d2
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
in dichloromethane
T=0°C; 0.0833333 h; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
tetrabutyl-ammonium chloride
1.) 60 deg C, 6 h, 2.) 80 deg C, 64 h; Yield given. Multistep reaction;
参考文献
Shibata, Ikuya; Yoshida, Tomoyuki; Baba, Akio; Matsuda, Haruo
Chemistry Letters, 1991 , # 2 p. 307 - 310
反应条件
in dichloromethane
T=0°C; 0.0833333 h; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
sodium perchlorate; water in acetonitrile
T=25°C; Hydrolysis; KineticsThermodynamic data; Further Variations:Temperatures;
参考文献
Bhat, J. Ishwara; Clegg, William; Maskill, Howard; Elsegood, Mark R.J.; Menneer, Iain D.; Miatt, Peter C.
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 7 p. 1435 - 1446
参考文献
Cornubert; Le Bihan
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 77
参考文献
Schorigin
Chemische Berichte, 1925 , vol. 58, p. 2033
