1-丁氧基-3-氯-2-丙醇合成路线 （共 11 条）
反应条件
zinc(II) chloride T=110 - 120°C; 2.5 h;
参考文献
Farzaliev, V. M.; Allakhverdiev, M. A.; Khalilova, A. Z.; Guseinova, T. M.
Russian Journal of Applied Chemistry, 1994 , vol. 67, # 6.2 p. 934
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1994 , vol. 67, # 6 p. 1049
反应条件
chromium (III) ethanoate T=80.05°C; Addition; KineticsActivation energyProduct distribution; Further Variations:Temperatures;
参考文献
Bukowski, Wiktor
International Journal of Chemical Kinetics, 2000 , vol. 32, # 6 p. 378 - 387
反应条件
tin(IV) chloride Rate constant;
参考文献
Drugov, M. V.; Barantsevich, E. N.; Smirnov P. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1052 - 1056
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1157 - 1162
反应条件
1: NaOH 2: 68 percent / aq. ethanol 3: 50 percent / butan-2-one / Heating View Scheme
参考文献
Stankyavichene, L. M. M.; Raizhene, D. I. L.; Vizas, V. K.; Stankyavichyus, A. P.; Terent'ev, P. B.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 5 p. 323 - 328
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 5 p. 548 - 553
反应条件
sodium hydroxide 10 h; Ambient temperature;
参考文献
Aiiakhverdiev; Farzaliev; Mustafaev
Russian Journal of Applied Chemistry, 1999 , vol. 72, # 9 p. 1660 - 1660
参考文献
Ponomarew; Polosuchina
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 1638; engl. Ausg. S. 1717
反应条件
1: aq. NaOH / 3 h / 60 - 70 °C 2: 128 g / thiourea / H2O / 2 h / 50 °C View Scheme
参考文献
Aiiakhverdiev; Farzaliev; Mustafaev
Russian Journal of Applied Chemistry, 1999 , vol. 72, # 9 p. 1660 - 1660
反应条件
1: satd. aq. NaOH / 10 h / Ambient temperature
2: 72 percent HClO4 / H2O / 12 h / 80 °C
3: 1.) Li-tert-butoxid, 2.) LiBr*H2O / 1.) tert-Butanol, reflux, 2.) reflux, ca. 12 d
View Scheme
参考文献
Gloe, K.; Muehl, P.; Beger, J.; Poeschmann, C.; Petrich, M.; Beyer, L.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 413 - 421
反应条件
(i) Na, toluene, (ii) /BRN= 1698575/; Multistep reaction;
参考文献
Fauran,C. et al.
Bulletin de la Societe Chimique de France, 1964 , p. 831 - 835
反应条件
1: satd. aq. NaOH / 10 h / Ambient temperature
2: 72 percent HClO4 / H2O / 12 h / 80 °C
View Scheme
参考文献
Gloe, K.; Muehl, P.; Beger, J.; Poeschmann, C.; Petrich, M.; Beyer, L.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 413 - 421
