Ethyl 2-(Diethoxyphosporyl)-2-hydroxyacetate合成路线 （共 4 条）
反应条件
toluene-4-sulfonic acid in water; toluene 12 h; Reflux;
参考文献
SHIONOGI andamp;; CO., LTD.; MIKAMIYAMA, Hidenori; MATSUMURA, Akira; MASUI, Moriyasu; ANAN, Kosuke; HATA, Kayoko
Patent: WO2010/114181 A1, 2010 ;
Location in patent: Page/Page column 93 ;
WO 2010/114181 A1
参考文献
Schmidt; Langner; Kirschbaum; Braun
Synthesis, 1994 , # 11 p. 1138 - 1140
反应条件
pyridine in dichloromethane T=0°C;
参考文献
Schmidt; Langner; Kirschbaum; Braun
Synthesis, 1994 , # 11 p. 1138 - 1140
反应条件
in toluene T=20°C; 12 h;
参考文献
Helmboldt, Hannes; Koehler, Daniel; Hiersemann, Martin
Organic Letters, 2006 , vol. 8, # 8 p. 1573 - 1576
