5-氯甲基呋喃-2-甲醛合成路线 (共 59 条)
参考文献
Sumitomo Chemical Company, Limited
Patent: US4335049 A1, 1982 ;
反应条件
triethylamine; sodium iodide in tetrahydrofuran 10 h; Yield given. Title compound not separated from byproducts;
参考文献
Klein, Larry L.; Shanklin, Michael S.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5202 - 5209
参考文献
Fenton; Gostling
Journal of the Chemical Society, 1901 , vol. 79, p. 814
参考文献
Green Chemistry, , vol. 12, # 3 p. 370 - 373
反应条件
palladium 10 on activated carbon; hydrogen in propan-1-ol T=60°C; P=760.051 Torr; pH=2.5; 1.5 h;
参考文献
Luijkx, Gerard C.A.; Huck, Nina P.M.; Van Rantwijk, Fred; Maat, Leendert; Van Bekkum, Herman
Heterocycles, 2009 , vol. 77, # 2 p. 1037 - 1044
反应条件
hydrogenchloride; 5 Pd(II)/C(eggshell); hydrogen in water; benzene T=90°C; P=15514.9 Torr; 1 h; Autoclave;
参考文献
ChemSusChem, , vol. 4, # 3 p. 349 - 352
反应条件
palladium on activated charcoal; hydrogen
参考文献
Mascal, Mark; Nikitin, Edward B.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 41 p. 7924 - 7926
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 1.2: 20 °C / Inert atmosphere 2.1: methanol / 1 h / 20 °C 2.2: 0.58 h / 0 - 20 °C 3.1: sodium hydroxide / water / 2 h / Reflux View Scheme
参考文献
Mascal, Mark; Dutta, Saikat
Green Chemistry, 2011 , vol. 13, # 11 p. 3101 - 3102
反应条件
1: diethyl ether 2: aluminium isopropylate; isopropyl alcohol View Scheme
参考文献
Gill; Ing
Journal of the Chemical Society, 1958 , p. 4728,4731
反应条件
potassium carbonate in acetonitrile T=20°C; 5 h;
参考文献
Kim, Jung-Keun; Kim, Se-Won; Oh, Kwi-Ok; Ko, Seon Yle; Kim, Jong Yeo; Lee, Byung-Eui; Kim, Bum Tae; Lee, Yeon Soo; Min, Yong Ki; Park, No Kyun
Patent: US2008/221205 A1, 2008 ;
Location in patent: Page/Page column 5-6 ;