1,1,2,2-四苯基二硅烷合成路线 （共 18 条）
反应条件
[Rh(i-Pr3P)2]OTf in deuterated toluene T=0°C; 24 h;
参考文献
Goikhman, Roman; Milstein, David
Chemistry - A European Journal, 2005 , vol. 11, # 10 p. 2983 - 2988
反应条件
titanium tetrachloride; zinc in tetrahydrofuran 24 h; Heating;
参考文献
Lai, Guoqiao; Li, Zhifang; Huang, Jiabang; Jiang, Jianxiong; Qiu, Huayu; Shen, Yongjia
Journal of Organometallic Chemistry, 2007 , vol. 692, # 16 p. 3559 - 3562
反应条件
(diphenyl)bis(.eta.5-cyclopentadienyl)titanium T=110°C; 24 h;
参考文献
Chemistry Letters, , p. 83 - 86
反应条件
tetramethyldialuminoxane; zirconium bis(benzimidinate) dimethyl T=90°C; 4 h;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 10 p. 1940 - 1950
反应条件
Mg-anode; stainless steel cathode in tetrahydrofuran 240 h; Electrolysis;
参考文献
Grogger, Christa; Loidl, Bernhard; Stueger, Harald; Kammel, Thomas; Pachaly, Bernd
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 105 - 110
反应条件
trichlorosilane; magnesium; methyl iodide 2.) THF, 72 h, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 538, # 1-2 p. 135 - 143
反应条件
in benzene-d6; benzene byproducts: CH4; (N2), dried solvents, room temp., gas evolution (2.5 h), color: orange; GC, identified by (29)Si-, (1)H-, (31)P-NMR, not isolated, rapid decompn.;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 165 - 172
反应条件
bromine in tetrachloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Gudnason, Palmar I.; Arnason, Ingvar
Organic Letters, 2009 , vol. 11, # 9 p. 2015 - 2017
反应条件
cesium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=100°C; 0.0833333 h;
参考文献
Tetrahedron Letters, , vol. 39, # 3-4 p. 171 - 174
反应条件
hydrogen; Wilkinson's catalyst in benzene-d6
参考文献
Journal of the American Chemical Society, , vol. 123, # 21 p. 5120 - 5121
