1,1,2,2-四苯基二硅烷合成路线 （共 18 条）
反应条件
Yb(η2-Ph2CN(C6H5))(hmpa)4 in tetrahydrofuran 17 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 63, # 25 p. 9265 - 9269
反应条件
trans-Pt(SiHPh2)2(PEt3)2; C24H42P2PtSi in benzene-d6 50 h; Schlenk techniqueAutoclave;
参考文献
Voigt, Jan; Chilleck, Maren A.; Braun, Thomas
Dalton Transactions, 2013 , vol. 42, # 11 p. 4052 - 4058
反应条件
hydrogen; Wilkinson's catalyst in benzene-d6
参考文献
Journal of the American Chemical Society, , vol. 123, # 21 p. 5120 - 5121
反应条件
aluminum triiodide in benzene dissolving disilane in C6H6; addn. of AlI3; vigorous stirring and addn. of dry HI; fractionation; elem. anal.;
参考文献
Hassler, K.; Poeschl, M.
Journal of Organometallic Chemistry, 1990 , vol. 398, # 3 p. 225 - 227
反应条件
HI in benzene dissolving of 1,1,2,2-diphenyldisilane in dry benzene; addn. of AlI3 and passing of a stream of dry HI through the soln.;; distillation;;
参考文献
Roehmen, Eirik; Hagen, Kolbjoern; Stoelevik, Reidar; Hassler, Karl; Poeschl, M.
Journal of Molecular Structure, 1991 , vol. 244, p. 41 - 49
反应条件
phosphorus pentachloride in tetrachloromethane
参考文献
Mawaziny,S.
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, 1970 , p. 1641 - 1642
反应条件
cesium fluoride in various solvent(s) T=100°C; 0.0833333 h;
参考文献
Lachance, Nicolas; Gallant, Michel
Tetrahedron Letters, 1998 , vol. 39, # 3-4 p. 171 - 174
反应条件
1: [Yb(η2-Ph2CNPh)(hmpa)3] / tetrahydrofuran
2: 16 percent Chromat. / [Yb(η2-Ph2CNPh)(hmpa)3] / tetrahydrofuran / 20 h / 20 °C
View Scheme
参考文献
Takaki, Ken; Komeyama, Kimihiro; Takehira, Katsuomi
Tetrahedron, 2003 , vol. 59, # 52 p. 10381 - 10395
