DL-2-氨基-3-甲基-1-丁醇合成路线 (共 25 条)
反应条件
zirconium(IV) borohydride in tetrahydrofuran T=25°C; Reduction; 3 h;
参考文献
Narasimhan; Balakumar
Synthetic Communications, 2000 , vol. 30, # 23 p. 4387 - 4395
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Aldrich-Boranes, Inc.
Patent: US3935280 A1, 1976 ;
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1230 - 1236
反应条件
N-(2-Aminoethyl)aminomethyl polystyrene in tetrahydrofuran T=60°C;
参考文献
Katz, Steven J; Bergmeier, Stephen C
Tetrahedron Letters, 2002 , vol. 43, # 4 p. 557 - 559
反应条件
lithium aluminium tetrahydride
参考文献
Chang, Zen-Yu; Coates, Robert M.
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3464 - 3474
反应条件
sodium hydroxide; sulfuric acid in tetrahydrofuran; diethyl ether
反应条件
sodium tetrahydroborate; iodine in tetrahydrofuran 4 h; Heating;
参考文献
Periasamy, Mariappan; Sivakumar, Sangarappan; Reddy, Meda Narsi
Synthesis, 2003 , # 13 p. 1965 - 1967
反应条件
sodium in propan-1-ol 1 h; Heating;
参考文献
Moody, Harold M.; Kaptein, Bernard; Broxterman, Quirinus B.; Boesten, Wilhelmus H. J.; Kamphuis, Johan
Tetrahedron Letters, 1994 , vol. 35, # 11 p. 1777 - 1780
反应条件
hydrogenchloride; iron T=100°C;
参考文献
Journal of the Chemical Society, , p. 410,414
参考文献
Journal of the Chemical Society, , p. 410,414