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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丁基铵乙酸盐
合成路线
（共 9 条）
64-19-7
醋酸
+
109-73-9
正丁胺
→
反应条件
1641-36-7
丁基铵乙酸盐
反应条件
T=0°C;
参考文献
McCrary, Parker D.; Beasley, Preston A.; Gurau, Gabriela; Narita, Asako; Barber, Patrick S.; Cojocaru, O. Andreea; Rogers, Robin D.
New Journal of Chemistry, 2013 , vol. 37, # 7 p. 2196 - 2202
1641-36-7
丁基铵乙酸盐
+
100-47-0
苯甲腈
→
反应条件
1575-95-7
N-乙酰基-苯甲酰胺
+
55-21-0
苯甲酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: benzonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
623-03-0
对氯苯甲腈
+
1641-36-7
丁基铵乙酸盐
→
反应条件
30334-17-9
+
619-56-7
4-氯苯甲酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: para-chloro-benzonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
1641-36-7
丁基铵乙酸盐
+
75-05-8
乙腈
→
反应条件
625-77-4
二乙酰基胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: acetonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
623-03-0
对氯苯甲腈
+
1641-36-7
丁基铵乙酸盐
→
反应条件
30334-17-9
+
619-56-7
4-氯苯甲酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: para-chloro-benzonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
140-29-4
氰化苄
+
1641-36-7
丁基铵乙酸盐
→
反应条件
10543-56-3
+
103-81-1
2-苯乙酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: phenylacetonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Tetrahedron Letters, , vol. 53, # 23 p. 2881 - 2884
140-29-4
氰化苄
+
1641-36-7
丁基铵乙酸盐
→
反应条件
10543-56-3
+
103-81-1
2-苯乙酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: phenylacetonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
1641-36-7
丁基铵乙酸盐
+
100-47-0
苯甲腈
→
反应条件
1575-95-7
N-乙酰基-苯甲酰胺
+
55-21-0
苯甲酰胺
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: benzonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
555-21-5
对硝基苯乙腈
+
1641-36-7
丁基铵乙酸盐
→
反应条件
反应条件
1: n-butylammonium acetate With trifluoromethylsulfonic anhydride T=0 - 20°C; 0.0833333 h; 2: (4-nitro-phenyl)-acetonitrile T=60°C; Ritter type reaction; 1 h; 3: With water; sodium hydrogencarbonate Ritter type reaction;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2881 - 2884
